1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate

Base Information

Chemical Name:1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate
CAS No.:950771-93-4
Molecular Formula:C₁₉H₃₆N₂O₃
Molecular Weight:340.506
Hs Code.:

Synonyms:1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate

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Chemical Property of 1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate

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Technology Process of 1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate

There total 3 articles about 1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69697-46-7
4-(propan-2-yloxy)cyclohexanone

: 73874-95-0
(piperidin-4-yl)carbamic acid tert-butyl ester

: 950771-93-4
1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate

Guidance literature:: 4-(propan-2-yloxy)cyclohexanone; tert‐butyl piperidin‐4‐ylcarbamate; With sodium tris(acetoxy)borohydride; In dichloromethane; at 20 ℃; for 18.1667h;

With methanol; In dichloromethane; for 0.333333h;

Reference yield:

: 22428-87-1
4,4-ethylenedioxycyclohexan-1-ol

: 950771-93-4
1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver(l) oxide / 288 h / 20 °C

2.1: sodium tris(acetoxy)borohydride / dichloromethane / 18.17 h / 20 °C

2.2: 0.33 h

With sodium tris(acetoxy)borohydride; silver(l) oxide; In dichloromethane;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 950771-93-4
1,1-dimethylethyl (1-{trans-4-[(1-methylethyl)oxy]cyclohexyl}-4-piperidinyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / ethanol / 1 h / 0 - 20 °C

2.1: silver(l) oxide / 288 h / 20 °C

3.1: sodium tris(acetoxy)borohydride / dichloromethane / 18.17 h / 20 °C

3.2: 0.33 h

With sodium tetrahydroborate; sodium tris(acetoxy)borohydride; silver(l) oxide; In ethanol; dichloromethane;