((CH₃)3Si)3CPb(CH₃)3

Base Information

• Chemical Name: ((CH₃)3Si)3CPb(CH₃)3
• CAS No.: 82289-21-2
• Molecular Formula: C₁₃H₃₆PbSi₃
• Molecular Weight: 483.885
• Mol file: 82289-21-2.mol

Synonyms:((CH₃)3Si)3CPb(CH₃)3

Chemical Property of ((CH₃)3Si)3CPb(CH₃)3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ((CH₃)3Si)3CPb(CH₃)3

There total 1 articles about ((CH₃)3Si)3CPb(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Pb(methyl)2(tris(trimethylsilyl)methyl)(8-hydroxyquinolinato)] → {Pb(C9H6NO)2} (14976-96-6) + [Pb(methyl)3(8-hydroxyquinolinato)] + [Pb(methyl)2(8-hydroxyquinolinato)2] (29345-86-6) + ((CH3)3Si)3CPb(CH3)3 (82289-21-2)

Guidance literature:

In methanol; benzene-d6; 70°C, 6 h; products not isolated; detected by NMR;

Reference yield: 90.0%

((CH3)3Si)3CPb(CH3)3 (82289-21-2) + tin(IV) chloride (7646-78-8) → dichloro(methyl)(tris(trimethylsilyl)methyl)lead(IV) (82289-23-4) + methyltin(IV) trichloride (993-16-8)

Guidance literature:

In benzene; SnCl4 was added dropwise to a soln. of Pb-compound in C6H6, stood for 1h; vac. sublimated, recrystd. from C6H6; elem. anal.;

DOI:10.1016/S0020-1693(00)90238-X

Reference yield:

formic acid (64-18-6) + ((CH3)3Si)3CPb(CH3)3 (82289-21-2) → lead(II) formate (811-54-1,7056-83-9)

Guidance literature:

In benzene; byproducts: CO2, CH4, ((CH3)3Si)3CH; Pb-compound was heated with an excess of formic acid in C6H6 at 100°C, further by-products; elem. anal.;

DOI:10.1016/S0020-1693(00)90238-X

Downstream raw materials:

lead(II) formate

dichloro(methyl)(tris(trimethylsilyl)methyl)lead(IV)

methyltin(IV) trichloride

PbCl(CH₃)2(C(Si(CH₃)3)3)