2-(TRIMETHYLSILYL)-6-METHOXYNAPHTHALENE

Base Information

• Chemical Name: 2-(TRIMETHYLSILYL)-6-METHOXYNAPHTHALENE
• CAS No.: 18410-39-4
• Molecular Formula: C₁₄H₁₈OSi
• Molecular Weight: 230.382
• Mol file: 18410-39-4.mol

Synonyms:(6-methoxynaphthalen-2-yl)trimethylsilane

Chemical Property of 2-(TRIMETHYLSILYL)-6-METHOXYNAPHTHALENE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

2-(TRIMETHYLSILYL)-6-METHOXYNAPHTHALENE ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(TRIMETHYLSILYL)-6-METHOXYNAPHTHALENE

There total 5 articles about 2-(TRIMETHYLSILYL)-6-METHOXYNAPHTHALENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

chloro-trimethyl-silane (75-77-4) + 2-lithio-6-methoxynaphthalene (32725-08-9) → (6-methoxynaphthalen-2-yl)trimethylsilane (18410-39-4)

Guidance literature:

In not given;

DOI:10.1021/ja01167a009

Reference yield:

2-Bromo-6-methoxynaphthalene (5111-65-9) → (6-methoxynaphthalen-2-yl)trimethylsilane (18410-39-4)

Guidance literature:

With n-butyllithium; folgende Umsetzung mit Chlor-trimethyl-silan;

DOI:10.1021/ja01167a009

Reference yield:

6-bromo-naphthalen-2-ol (15231-91-1) → (6-methoxynaphthalen-2-yl)trimethylsilane (18410-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: butyl lithium / folgende Umsetzung mit Chlor-trimethyl-silan

With n-butyllithium;

DOI:10.1021/ja01167a009

upstream raw materials:

2-Bromo-6-methoxynaphthalene

6-(trimethylsilyl)naphthalen-2-ol

dimethyl sulfate

6-bromo-naphthalen-2-ol

Downstream raw materials:

trimethyl(6-phenylnaphthalen-2-yl)silane

2-naphthyltrimethylsilane

Refernces