3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate

Base Information

Chemical Name:3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate
CAS No.:511295-06-0
Molecular Formula:C₁₂H₁₂ClF₃O₆S
Molecular Weight:376.738
Hs Code.:

Synonyms:3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate

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Chemical Property of 3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate

Chemical Property:

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Technology Process of 3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate

There total 5 articles about 3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 511295-25-3
3-chloro-5-[1,3]dioxan-2-yl-2-methoxy-phenol

: 511295-06-0
3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1055/s-2002-35629

Reference yield:

: 621-59-0
isovanillin

: 511295-06-0
3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / 1 h / Heating

2: 79 percent / N,N'-dichloropiperazine / aq. H₂SO₄ / 1 h / 20 °C

3: 95 percent / aq. NaOH / 2 h / Heating

4: 96 percent / p-TosOH / toluene / 24 h / Heating

5: 68 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

With pyridine; N,N'-dichloropiperazine; sodium hydroxide; toluene-4-sulfonic acid; In dichloromethane; sulfuric acid; toluene;
DOI:10.1055/s-2002-35629

Reference yield:

: 54246-06-9
3-chloro-5-hydroxy-4-methoxybenzaldehyde

: 511295-06-0
3-chloro-5-(1,3-dioxan-2-yl)-2-methoxyphenyl trifluoromethane sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / p-TosOH / toluene / 24 h / Heating

2: 68 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

With pyridine; toluene-4-sulfonic acid; In dichloromethane; toluene;
DOI:10.1055/s-2002-35629