BrC₆H₄C₃H₅O₂CH₂

Base Information

• Chemical Name: BrC₆H₄C₃H₅O₂CH₂
• CAS No.: 937795-06-7
• Molecular Formula: C₁₀H₁₁BrO₂
• Molecular Weight: 243.1
• Mol file: 937795-06-7.mol

Synonyms:BrC₆H₄C₃H₅O₂CH₂

Chemical Property of BrC₆H₄C₃H₅O₂CH₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of BrC₆H₄C₃H₅O₂CH₂

There total 1 articles about BrC₆H₄C₃H₅O₂CH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

[(2S,3S)-3-(4-bromophenyl)oxiran-2-yl]methanol (106948-05-4) + methyl iodide (74-88-4) → BrC6H4C3H5O2CH2 (937795-06-7)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at -20 - 20 ℃;

DOI:10.1021/jo062612t

Reference yield: 84.0%

BrC6H4C3H5O2CH2 (937795-06-7) + 2-Methylphenylboronic acid (16419-60-6) → C16H14O2CH4 (937795-17-0)

Guidance literature:

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate; [Pd₂(dba)₃]*benzene; In toluene; at 100 ℃; for 0.75h;

DOI:10.1021/jo062612t

Reference yield: 84.0%

BrC6H4C3H5O2CH2 (937795-06-7) + 3,5-bis-trifluromethylphenylboronic acid (73852-19-4) → C16H14O2(CF3)2 (937795-14-7)

Guidance literature:

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate; [Pd₂(dba)₃]*benzene; In toluene; at 100 ℃; for 0.5h;

DOI:10.1021/jo062612t

upstream raw materials:

[(2S,3S)-3-(4-bromophenyl)oxiran-2-yl]methanol

methyl iodide

Downstream raw materials:

C₁₆H₁₆O₂

C₁₆H₁₄O₂(CF₃)2

C₁₆H₁₄O₂(CH₃)2

C₁₆H₁₄O₂CH₄O

Refernces