[(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Zn(II)(3-hydroxyflavonolate)](triflate)

Base Information

Chemical Name:[(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Zn(II)(3-hydroxyflavonolate)](triflate)
CAS No.:1202525-28-7
Molecular Formula:CF₃O₃S*C₄₅H₃₅N₄O₃Zn
Molecular Weight:894.258
Hs Code.:

Synonyms:[(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Zn(II)(3-hydroxyflavonolate)](triflate)

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Chemical Property of [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Zn(II)(3-hydroxyflavonolate)](triflate)

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Technology Process of [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Zn(II)(3-hydroxyflavonolate)](triflate)

There total 1 articles about [(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Zn(II)(3-hydroxyflavonolate)](triflate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 577-85-5,66585-05-5
3-hydroxyflavone

: 167897-42-9
N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)-methyl)amine

: 54010-75-2
zinc trifluoromethanesulfonate

: 1202525-28-7
[(N,N-bis((6-phenyl-2-pyridyl)methyl)-N-((2-pyridyl)methyl)amine)Zn(II)(3-hydroxyflavonolate)](triflate)

Guidance literature:: With tetramethylammonium hydroxide pentahydrate; In methanol; byproducts: (Me4N)(SO3CF3); under N2; MeOH soln. of Zn salt added to solid amine; stirred until the amine dissolved; added to MeOH soln. contg. 3-hydroxyflavonol and Me4NOH*5H2O; stirred at ambient temp. overnight; solvent removed under reduced pressure; suspended on top of Celite plug;washed (distd. H2O); dissolved in CH2Cl2; filtrate collected; brought t o dryness under reduced pressure; dissolved in CH2Cl2; Et2O added; cooled (-30.degrede.C, 12 h); elem. anal.;
DOI:10.1021/ic901405h