Technology Process of 2-phenylpentanedinitrile
There total 9 articles about 2-phenylpentanedinitrile which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-benzyl-trimethylammonium hydroxide;
In
1,4-dioxane; methanol;
for 15h;
Heating;
DOI:10.1021/jm00158a007
- Guidance literature:
-
With
tetrakis(acetonitrile)copper(I) hexafluorophosphate; 10-phenyl-10H-phenothiazine; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
N,N-dimethyl acetamide;
at 30 ℃;
Schlenk technique;
Inert atmosphere;
Irradiation;
DOI:10.1021/acs.orglett.9b03970
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 0 °C
2: sodium acetate; hydroxylamine hydrochloride / methanol / 3 h / 75 °C
3: triethylamine / dichloromethane / 1 h / 0 °C
4: 4,4'-di-tert-butyl-2,2'-bipyridine; 10-phenyl-10H-phenothiazine; tetrakis(acetonitrile)copper(I) hexafluorophosphate / N,N-dimethyl acetamide / 30 °C / Schlenk technique; Inert atmosphere; Irradiation
With
tetrakis(acetonitrile)copper(I) hexafluorophosphate; 10-phenyl-10H-phenothiazine; hydroxylamine hydrochloride; sodium acetate; triethylamine; 3-chloro-benzenecarboperoxoic acid; 4,4'-di-tert-butyl-2,2'-bipyridine;
In
methanol; dichloromethane; N,N-dimethyl acetamide;
DOI:10.1021/acs.orglett.9b03970
