di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium

Base Information

Chemical Name:di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium
CAS No.:81835-23-6
Molecular Formula:C₄₆H₄₄O₆P₂Ru
Molecular Weight:855.869
Hs Code.:

Synonyms:di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium

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Chemical Property of di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium

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Technology Process of di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium

There total 5 articles about di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 27599-25-3,54083-06-6,19529-00-1
dihydridotetrakis(triphenylphosphine)ruthenium

: 123-72-8
butyraldehyde

: Ru(OCOC₃H₇)2(CO)(P(C₆H₅)3)2

: 81835-23-6
di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium

Guidance literature:: With water; In neat (no solvent); PrCHO and water added to Ru complex in vac., heated at 110°C in vac. for 2 h, cooled to room temp.; crystals filtered, washed with Et2O and hexane, dried in vac.; elem. anal.;
DOI:10.1246/bcsj.55.504

Reference yield: 30.0%

: 27599-25-3,54083-06-6,19529-00-1
dihydridotetrakis(triphenylphosphine)ruthenium

: 123-72-8
butyraldehyde

: 81835-23-6
di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium

: 109-21-7
butyl butyrate

: 201230-82-2
carbon monoxide

: 1333-74-0
hydrogen

: 71-36-3
butan-1-ol

Guidance literature:: With water; In neat (no solvent); byproducts: propane, propene; PrCHO and water added to Ru complex in vac., heated at 110°C in vac. for 2 h; evapd. in vac., solid washed with Et2O and hexane, recrystd. from toluene, dried in vac.; elem. anal.;
DOI:10.1246/bcsj.55.504

Reference yield:

: 25087-79-0
RuH(OCOC₃H₇)(P(C₆H₅)3)3

: 123-72-8
butyraldehyde

: 81835-23-6
di(butyrato)dicarbonylbis(triphenylphosphine)ruthenium

: 109-21-7
butyl butyrate

: 201230-82-2
carbon monoxide

: 1333-74-0
hydrogen

: 71-36-3
butan-1-ol

Guidance literature:: With water; In neat (no solvent); PrCHO and water added to Ru complex in vac., heated at 110°C in vac. for 2 h; evapd. in vac., solid washed with Et2O and hexane, recrystd. from toluene, dried in vac.;
DOI:10.1246/bcsj.55.504