4-[[(Phenylamino)carbonyl]amino]benzenesulfonyl chloride

Base Information

Chemical Name:4-[[(Phenylamino)carbonyl]amino]benzenesulfonyl chloride
CAS No.:203640-35-1
Molecular Formula:C₁₃H₁₁ClN₂O₃S
Molecular Weight:310.761
Hs Code.:
DSSTox Substance ID:DTXSID901202753
ChEMBL ID:CHEMBL2436676

Synonyms:CHEMBL2436676;SCHEMBL12011007;DTXSID901202753;BDBM50493722;4-[[(Phenylamino)carbonyl]amino]benzenesulfonyl chloride;203640-35-1

Suppliers and Price of 4-[[(Phenylamino)carbonyl]amino]benzenesulfonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[[(Phenylamino)carbonyl]amino]benzenesulfonyl chloride

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:310.0178911
Heavy Atom Count:20
Complexity:421

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=O)NC2=CC=C(C=C2)S(=O)(=O)Cl

Technology Process of 4-[[(Phenylamino)carbonyl]amino]benzenesulfonyl chloride

There total 4 articles about 4-[[(Phenylamino)carbonyl]amino]benzenesulfonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 6752-38-1
4-chlorosulfonylbenzene isocyanate

: 62-53-3
aniline

: 203640-35-1
4-[(anilinocarbonyl)amino]benzenesulfonyl chloride

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 1.5h;
DOI:10.1021/jm9707582

Reference yield: 47.0%

: 24939-24-0
4-aminobenzenesulfonyl chloride

: 103-71-9
phenyl isocyanate

: 203640-35-1
4-[(anilinocarbonyl)amino]benzenesulfonyl chloride

Guidance literature:: In ethanol; for 13h; Reflux;
DOI:10.1016/j.ejmech.2013.07.040

Reference yield:

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 203640-35-1
4-[(anilinocarbonyl)amino]benzenesulfonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrazine hydrate / ethanol / 0.33 h / 100 °C / Microwave irradiation

2: ethanol / 13 h / Reflux

With palladium on activated charcoal; hydrazine hydrate; In ethanol;
DOI:10.1016/j.ejmech.2013.07.040