C₁₇H₁₈O₂

Base Information

Chemical Name:C₁₇H₁₈O₂
CAS No.:1337920-89-4
Molecular Formula:C₁₇H₁₈O₂
Molecular Weight:254.329
Hs Code.:

C<sub>17</sub>H<sub>18</sub>O<sub>2</sub>

Synonyms:C₁₇H₁₈O₂

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Chemical Property of C₁₇H₁₈O₂

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Technology Process of C₁₇H₁₈O₂

There total 4 articles about C₁₇H₁₈O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 769-60-8
2-methyl-1-phenylprop-2-en-1-one

: C₁₇H₁₈O₂

: 1337920-89-4
C₁₇H₁₈O₂

: 3-hydroxy-2,2-dimethyl-1,3-diphenylpropyl benzoate

: 3-hydroxy-2,2-dimethyl-1,3-diphenylpropyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Wilkinson's catalyst / 0.5 h / 90 °C / Inert atmosphere

2.1: (R)-3,3'-dichloro-1,1'-binaphthalene-2,2'-diol lithium salt / tetrahydrofuran; hexane / 24 h / -45 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

With Wilkinson's catalyst; (R)-3,3'-dichloro-1,1'-binaphthalene-2,2'-diol lithium salt; In tetrahydrofuran; hexane;
DOI:10.1016/j.tet.2012.03.096

Reference yield:

: 1379003-24-3
2-methyl-1-phenyl-1-(trimethoxysilyloxy)-1-propene

: 100-52-7
benzaldehyde

: C₁₇H₁₈O₂

: 1337920-89-4
C₁₇H₁₈O₂

: 3-hydroxy-2,2-dimethyl-1,3-diphenylpropyl benzoate

: 3-hydroxy-2,2-dimethyl-1,3-diphenylpropyl benzoate

Guidance literature:: 2-methyl-1-phenyl-1-(trimethoxysilyloxy)-1-propene; benzaldehyde; With (R)-3,3'-dichloro-1,1'-binaphthalene-2,2'-diol lithium salt; In tetrahydrofuran; hexane; at -45 ℃; for 24h; Inert atmosphere;

With potassium fluoride; formic acid; In tetrahydrofuran; hexane; water; at 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2012.03.096

Reference yield:

: 75990-52-2
3-hydroxy-2,2-dimethyl-1,3-diphenylpropan-1-one

: 123-62-6
propionic acid anhydride

: 1337920-89-4
C₁₇H₁₈O₂

: C₂₀H₂₂O₃

: C₂₀H₂₂O₃

Guidance literature:: 3-hydroxy-2,2-dimethyl-1,3-diphenylpropan-1-one; With C₅₁H₄₀FeN₂; N-ethyl-N,N-diisopropylamine; In toluene; at 0 ℃; for 0.0833333h;

propionic acid anhydride; In toluene; at 0 ℃; for 93h; optical yield given as %ee;
DOI:10.1039/c1cc14591f