phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide

Base Information

Chemical Name:phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide
CAS No.:197631-81-5
Molecular Formula:C₁₆H₂₄O₆S
Molecular Weight:344.429
Hs Code.:

Synonyms:phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide

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Technology Process of phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide

There total 1 articles about phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 197631-83-7
phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside

: 197631-81-5
phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - -30 ℃; for 0.5h;
DOI:10.1021/ja971239r

Reference yield: 40.0%

: 67-56-1
methanol

: 197631-81-5
phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide

: 197631-83-7
phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside

: 3445-71-4
methyl-(tetra-O-methyl-β-D-mannopyranoside)

: 3149-62-0
methyl 2,3,4,6-tetra-O-methyl-α-D-mannopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; trifluoromethylsulfonic anhydride; Product distribution; multistep reaction;
DOI:10.1021/ja971239r

Reference yield:

: 197631-81-5
phenyl 2,3,4,6-tetra-O-methyl-1-deoxy-1-thio-α-D-mannopyranoside S-oxide

: 108-93-0
cyclohexanol

: cyclohexyl 2,3,4,6-tetra-O-methyl-β-D-mannopyranoside

: cyclohexyl 2,3,4,6-tetra-O-methyl-α-D-mannopyranoside

Guidance literature:: With zirconocene dichloride; 4 A molecular sieve; silver perchlorate; In dichloromethane; at -20 - 20 ℃; for 6h; Title compound not separated from byproducts.;
DOI:10.1021/jo015952h