7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline

Base Information

Chemical Name:7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline
CAS No.:620962-75-6
Molecular Formula:C₂₀H₁₅F₃N₂OS
Molecular Weight:388.413
Hs Code.:

Synonyms:7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline

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Chemical Property of 7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline

Chemical Property:

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Technology Process of 7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline

There total 4 articles about 7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 620962-74-5
N-(2-bromoquinolin-3-yl)methyl-N-[2,2-bis(phenylthio)ethenyl]trifluoroacetamide

: 620962-75-6
7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 4h; Heating;
DOI:10.1021/jo030177m

Reference yield:

: 35740-83-1
2-bromo-3-bromomethylquinoline

: 620962-75-6
7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / aq. NH₄OH / 120 h / 20 °C

2: 82 percent / MgSO₄ / diethyl ether / 10 h / 20 °C

3: 84 percent / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

4: 85 percent / Bu₃SnH; AIBN / benzene / 4 h / Heating

With ammonium hydroxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; magnesium sulfate; triethylamine; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo030177m

Reference yield:

: 292077-58-8
C-(2-Bromoquinolin-3-yl)methylamine

: 620962-75-6
7-trifluoroacetyl-6,8-dihydro-6-(phenylthiomethyl)pyrrolo[3,4-b]quinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / MgSO₄ / diethyl ether / 10 h / 20 °C

2: 84 percent / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

3: 85 percent / Bu₃SnH; AIBN / benzene / 4 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; magnesium sulfate; triethylamine; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo030177m