3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide

Base Information

Chemical Name:3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide
CAS No.:1268525-99-0
Molecular Formula:C₂₇H₃₄ClN₂*I
Molecular Weight:548.938
Hs Code.:

Synonyms:3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide

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Chemical Property of 3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide

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Technology Process of 3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide

There total 7 articles about 3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1268525-89-8
N-(4-chlorophenyl)-N-(5-cyclohexylpentyl)-quinolin-3-yl-amine

: 74-88-4
methyl iodide

: 1268525-99-0
3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide

Guidance literature:: In toluene; at 110 ℃; for 24h;
DOI:10.1016/j.bmc.2010.10.065

Reference yield:

: 931-50-0
cyclohexylmagnesium bromide

: 1268525-99-0
3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide

Guidance literature:: Multi-step reaction with 4 steps

1.1: dilithium tetrachlorocuprate / tetrahydrofuran; diethyl ether / 0.42 h / 5 - 10 °C / Inert atmosphere

1.2: 13.5 h / 0 - 20 °C

2.1: sodium iodide / acetone / 12 h / 60 °C

3.1: sodium hydride / 1,2-dimethoxyethane / 12 h / 20 °C

4.1: toluene / 24 h / 110 °C / Sealed tube

With dilithium tetrachlorocuprate; sodium hydride; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; acetone; toluene;

Reference yield:

: 1679-18-1
4-Chlorophenylboronic acid

: 1268525-99-0
3-((4-chlorophenyl)(5-cyclohexylpentyl)amino)-1-methylquinolinium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / copper diacetate / dichloromethane / 20 °C / Molecular sieve

2: sodium hydride / 1,2-dimethoxyethane / 12 h / 20 °C

3: toluene / 24 h / 110 °C / Sealed tube

With sodium hydride; triethylamine; copper diacetate; In 1,2-dimethoxyethane; dichloromethane; toluene;