ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

Base Information

Chemical Name:ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate
CAS No.:98314-81-9
Molecular Formula:C₃₀H₃₄O₁₀
Molecular Weight:554.594
Hs Code.:

Synonyms:ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

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Chemical Property of ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

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Technology Process of ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

There total 3 articles about ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 98314-80-8
ethyl 2-<4-formyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

: 149-73-5
trimethyl orthoformate

: 98314-81-9
ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

Guidance literature:: With ammonium chloride; In methanol; for 1h; Heating;
DOI:10.1248/cpb.33.1419

Reference yield:

: 65298-98-8
4-hydroxy-3-(methoxymethoxy)benzaldehyde

: 98314-81-9
ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / tert-BuOK / dimethylformamide / 3 h / Ambient temperature

2: 94 percent / NH₄Cl / methanol / 1 h / Heating

With potassium tert-butylate; ammonium chloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.33.1419

Reference yield:

: 7572-90-9
ethyl 2-bromo-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

: 98314-81-9
ethyl 2-<4-dimethoxymethyl-2-(methoxymethoxy)phenoxy>-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / tert-BuOK / dimethylformamide / 3 h / Ambient temperature

2: 94 percent / NH₄Cl / methanol / 1 h / Heating

With potassium tert-butylate; ammonium chloride; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.33.1419