6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine

Base Information

• Chemical Name: 6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine
• CAS No.: 1352804-07-9
• Molecular Formula: C₂₂H₃₁ClN₆O₂
• Molecular Weight: 446.98

Synonyms:6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine

Chemical Property of 6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine

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Technology Process of 6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine

There total 1 articles about 6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-(tert-butoxycarbonyl)-4-aminopiperidine (87120-72-7) + 4,6-dichloro-N-mesityl-1,3,5-triazin-2-amine → 6-chloro-N2-mesityl-N4-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine (1352804-07-9)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; water; acetone; at 30 ℃; for 8h;

DOI:10.1016/j.ejmech.2012.02.019

Reference yield: 96.0%

6-chloro-N2-mesityl-N4-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine (1352804-07-9) + methylamine (74-89-5) → N2-mesityl-N4-methyl-N6-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine (1352804-08-0)

Guidance literature:

With sodium hydrogencarbonate; In tetrahydrofuran; water; at 50 ℃; for 5h;

DOI:10.1016/j.ejmech.2012.02.019

Reference yield: 94.0%

methanol (67-56-1) + 6-chloro-N2-mesityl-N4-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine (1352804-07-9) → N2-mesityl-6-methoxy-N4-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine (1352804-09-1)

Guidance literature:

With sodium; at 60 ℃; for 4h;

DOI:10.1016/j.ejmech.2012.02.019

upstream raw materials:

1-(tert-butoxycarbonyl)-4-aminopiperidine

Downstream raw materials:

N₂-mesityl-6-methoxy-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine

N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

N₂-mesityl-N₄-methyl-N₆-(1-(4-nitrobenzyl)piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

N₂-(1-(4-fluorobenzyl)piperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

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