3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine

Base Information

Chemical Name:3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine
CAS No.:1395093-63-6
Molecular Formula:C₂₈H₂₄N₂O
Molecular Weight:404.511
Hs Code.:

Synonyms:3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine

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Chemical Property of 3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine

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Technology Process of 3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine

There total 4 articles about 3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1395093-61-4
3-(2,6-dibromophenyl)-11-methoxyimidazo[1,2-f]phenanthridine

: 126726-62-3
2-isopropenyl-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1395093-63-6
3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; toluene; for 18h; Reflux;

Reference yield:

: 191171-55-8
2-anilineboronic acid pinacol ester

: 1395093-63-6
3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium phosphate monohydrate / bis-triphenylphosphine-palladium(II) chloride / toluene; water / 15.5 h / Inert atmosphere

2.1: isopropyl alcohol / 24 h / Reflux

2.2: 24 h / 60 °C / Reflux

3.1: potassium phosphate monohydrate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; water / 18 h / Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; isopropyl alcohol; toluene;

Reference yield:

: 138642-47-4
2-bromo-5-methoxybenzonitrile

: 1395093-63-6
3-(2,6-diprop-1-en-2-ylphenyl)-11-methoxyimidazo[1,2-f]phenanthridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium phosphate monohydrate / bis-triphenylphosphine-palladium(II) chloride / toluene; water / 15.5 h / Inert atmosphere

2.1: isopropyl alcohol / 24 h / Reflux

2.2: 24 h / 60 °C / Reflux

3.1: potassium phosphate monohydrate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene; water / 18 h / Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In water; isopropyl alcohol; toluene;