Ga^III(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido))

Base Information

• Chemical Name: Ga^III(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido))
• CAS No.: 1422041-88-0
• Molecular Formula: C₃₃H₄₅GaN₄O₆S₃
• Molecular Weight: 759.664

Synonyms:Ga^III(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido))

Chemical Property of Ga^III(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido))

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Technology Process of Ga^III(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido))

There total 1 articles about Ga^III(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

gallium(III) trichloride + N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide) (1311297-64-9) → GaIII(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido)) (1422041-88-0)

Guidance literature:

N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide); With sodium hydride; In tetrahydrofuran; at 20 ℃; for 4h;

gallium(III) trichloride; In tetrahydrofuran; pentane; at 20 ℃; for 2h;

DOI:10.1039/c2sc21400h

Reference yield: 53.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + dichloromethane (75-09-2) + GaIII(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido)) (1422041-88-0) + ammonia (7664-41-7) → [GaIII(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido))(NH3)].0.75CH2Cl2.0.25THF

Guidance literature:

for 4h;

DOI:10.1039/c3cc48804g

Reference yield: 30.0%

GaIII(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido)) (1422041-88-0) + C10H20O5Sr(2+)*2CF3O3S(1-) + tetramethyl ammoniumhydroxide (75-59-2,104422-11-9,123626-97-1,154636-59-6,195460-17-4,78017-87-5,93615-68-0,129654-61-1) → C43H66GaN4O12S3Sr(1+)*CF3O3S(1-)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c2sc21400h

upstream raw materials:

N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)

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