2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine

Base Information

• Chemical Name: 2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine
• CAS No.: 86508-62-5
• Molecular Formula: C₈H₅Cl₃F₃N₂OP
• Molecular Weight: 339.468

Synonyms:2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine

Chemical Property of 2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine

Chemical Property:

Purity/Quality:

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Technology Process of 2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine

There total 3 articles about 2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,2,2-trifluoro-N′-phenylacetohydrazide (34064-31-8) → 2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ5-oxadiazaphospholine (86508-62-5)

Guidance literature:

With phosphorus pentachloride; In toluene; for 2h; Ambient temperature;

DOI:10.1246/cl.1983.507 DOI:10.1246/bcsj.57.2689

Reference yield:

phenylhydrazine (100-63-0) → 2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ5-oxadiazaphospholine (86508-62-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent

2: 93 percent / PCl₅ / toluene / 2 h / Ambient temperature

With phosphorus pentachloride; In toluene;

DOI:10.1246/cl.1983.507

Reference yield:

N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate (125972-09-0) → 2,2,2-Trichloro-3-phenyl-5-trifluoromethyl-1,3,4,2λ5-oxadiazaphospholine (86508-62-5)

Guidance literature:

Heating; distillation;

upstream raw materials:

2,2,2-trifluoro-N′-phenylacetohydrazide

N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate

phenylhydrazine

Downstream raw materials:

diethyl phosphorylchloridite

2-trifluoromethyl-4-phenyl-5-chloro-1,3,4,5-oxadiazaphospholine

N-α-Chlorotrifluoroacetylimino-N'-phenylhydrazidodichlorophosphate

2,2,2-Trifluoro-3-phenyl-5-trifluoromethyl-1,3,4,2λ⁵-oxadiazaphospholine

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