DIALLYLPHOSPHITE

Base Information

• Chemical Name: DIALLYLPHOSPHITE
• CAS No.: 23679-20-1
• Molecular Formula: C6H11 O3 P
• Molecular Weight: 162.125
• Hs Code.: 2920909090
• Mol file: 23679-20-1.mol

Synonyms:Allylphosphonate (6CI); Phosphonic acid, di-2-propenyl ester (9CI); Phosphonic acid,diallyl ester (8CI); Diallyl hydrogen phosphite; Diallyl phosphite; Diallylphosphonate; NSC 512600

Chemical Property of DIALLYLPHOSPHITE

Chemical Property:

• PSA: 52.28000
• Density: 1.0800
• LogP: 1.61080

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s): 3
• Hazard Codes: 3:
• Safety Statements: A poison. May explode during distillation. When heated to decomposition it emits t"> x. See also ALLYL COMPOUNDS." target="_blank">A poison. May explode during distillation. When heated to decomposition it emits t

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIALLYLPHOSPHITE

There total 2 articles about DIALLYLPHOSPHITE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

phenyl phosphorodichloridite (3426-89-9) + allyl alcohol (107-18-6) → diallyl phosphite (23679-20-1) + phenyl allyl H-phosphonate diester (164363-16-0)

Guidance literature:

With tert-butyl alcohol; In dichloromethane; at 20 ℃; for 0.333333h;

DOI:10.1055/s-2005-871580

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + triallyl phosphite (102-84-1) → diallyl phosphite (23679-20-1) + 3-chloroprop-1-ene (107-05-1)

Guidance literature:

Reference yield: 95.0%

piperonal (120-57-0,30024-74-9) + diallyl phosphite (23679-20-1) + aniline (62-53-3) → diallyl (benzo[d][1,3]dioxol-5-yl(phenylamino)methyl)phosphonate (1449479-34-8)

Guidance literature:

With Amberlite-IR 120; for 0.0333333h; Microwave irradiation;

DOI:10.1016/j.ejmech.2013.05.036

upstream raw materials:

hydrogenchloride

triallyl phosphite

phenyl phosphorodichloridite

allyl alcohol

Downstream raw materials:

bis(prop-2-en-1-yl)chlorophosphonate

(1-hydroxy-cyclohexyl)-phosphonic acid diallyl ester

3-(bis-allyloxy-phosphoryl)-3-phenyl-propionic acid ethyl ester

Acetic acid (bis-allyloxy-phosphoryl)-phenyl-methyl ester

Refernces