1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine

Base Information

Chemical Name:1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine
CAS No.:1643962-13-3
Molecular Formula:C₃₀H₄₈N₂Si
Molecular Weight:464.81
Hs Code.:

Synonyms:1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine

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Chemical Property of 1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine

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Technology Process of 1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine

There total 6 articles about 1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 75-77-4
chloro-trimethyl-silane

: 1643961-90-3
1-(4-bromo-2,6-diisopropylphenyl)-3-(2,6-diisopropylphenyl)imidazolidine

: 1643962-13-3
1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine

Guidance literature:: 1-(4-bromo-2,6-diisopropylphenyl)-3-(2,6-diisopropylphenyl)imidazolidine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at 20 ℃;
DOI:10.1002/ejoc.201402364

Reference yield:

: 80058-84-0
4-bromo-2,6-diisopropylaniline

: 1643962-13-3
1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane; N,N-dimethyl-formamide / 4 h / 20 °C

2.1: borane-tetrahydrofuran complex / Reflux

3.1: water; acetic acid / 12 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

4.2: 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201402364

Reference yield:

: 1643961-87-8
N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

: 1643962-13-3
1-[2,6-diisopropyl-4-(trimethylsilyl)phenyl]-3-(2,6-diisopropylphenyl)imidazolidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: borane-tetrahydrofuran complex / Reflux

2.1: water; acetic acid / 12 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

3.2: 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; water; acetic acid;
DOI:10.1002/ejoc.201402364