N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylglycine methyl ester

Base Information

Chemical Name:N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylglycine methyl ester
CAS No.:395647-17-3
Molecular Formula:C₂₃H₂₈N₄O₅
Molecular Weight:440.499
Hs Code.:

Synonyms:N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylglycine methyl ester

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Chemical Property of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylglycine methyl ester

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Technology Process of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylglycine methyl ester

There total 2 articles about N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylglycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 395647-10-6
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}glycine methyl ester

: 395647-17-3
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylglycine methyl ester

Guidance literature:: With dmap; In acetonitrile;
DOI:10.1016/S0040-4039(01)01350-8

Reference yield:

: 20691-84-3
m-methyl red

: 395647-17-3
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylglycine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / DCC; HOBt / dimethylformamide

2: 90 percent / DMAP / acetonitrile / 20 °C

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b212470j