methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate

Base Information

Chemical Name:methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate
CAS No.:177409-15-3
Molecular Formula:C₁₇H₂₀Cl₂N₄O₃
Molecular Weight:399.277
Hs Code.:

Synonyms:methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate

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Chemical Property of methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate

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Technology Process of methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate

There total 1 articles about methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 89088-56-2
methyl 1-methyl-3-aminopyrazole-5-carboxylate

: 15944-88-4
4-[N,N-bis(2-chloroethyl)amino]benzoyl chloride

: 177409-15-3
methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate

Guidance literature:: With TEA; In 1,4-dioxane; Ambient temperature;
DOI:10.1016/S0968-0896(98)00205-3

Reference yield: 84.0%

: 177409-15-3
methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate

: 177409-16-4
1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylic acid

Guidance literature:: With potassium hydroxide; In 1,4-dioxane; for 2h; Ambient temperature;
DOI:10.1016/S0968-0896(98)00205-3

Reference yield:

: 177409-15-3
methyl 1-methyl-4-<4-bis(2-chloroethyl)aminophenylamido>pyrazole-5-carboxylate

: 223437-72-7
3-<1-methyl-3-<1-methyl-3-<1-methyl-3-<4-bis(2-chloroethyl)aminophenylamido>-pyrazole-5-carboxamido>pyrazole-5-carboxamido>>pyrazole-5-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / aq. KOH / dioxane / 2 h / Ambient temperature

2: HOBt, EDC / dimethylformamide / 12 h / Ambient temperature

3: 100 percent / aq. KOH / dioxane / 2 h / Ambient temperature

With potassium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(98)00205-3