SY₆₃₄-70AP₁

Base Information

Chemical Name:SY₆₃₄-70AP₁
CAS No.:1269040-80-3
Molecular Formula:C₄₇H₆₈N₂O₁₅
Molecular Weight:901.061
Hs Code.:

Synonyms:SY₆₃₄-70AP₁

Suppliers and Price of SY₆₃₄-70AP₁

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Chemical Property of SY₆₃₄-70AP₁

Chemical Property:

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Technology Process of SY₆₃₄-70AP₁

There total 11 articles about SY₆₃₄-70AP₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1269040-79-0
C₄₅H₆₁NO₁₆

: 124-40-3
dimethyl amine

: 1269040-80-3
SY₆₃₄-70AP₁

Guidance literature:: With sodium cyanoborohydride; acetic acid; In ethanol; at 20 ℃; for 2.33333h;

Reference yield:

: 92950-45-3
10-dehydro 10-deacetyl 7-epibaccatin V

: 1269040-80-3
SY₆₃₄-70AP₁

Guidance literature:: Multi-step reaction with 10 steps

1.1: pyridine / -20 - 5.8 °C / Inert atmosphere

1.2: -17.5 - 20 °C

2.1: lithium borohydride / ethanol; tetrahydrofuran / -12 - 15 °C / Inert atmosphere

2.2: -10.8 - -3 °C

3.1: dmap; triethylamine / Isopropyl acetate / 3 h / 35 °C / Inert atmosphere

3.2: 0.25 h / 19.7 °C

4.1: water / acetic acid / methanol / 9 h / 50 - 55 °C

5.1: trifluoroacetic acid / toluene / -15 °C

5.2: 0.25 h / 5 °C / pH > 5

6.1: dmap; pivaloyl chloride; 4-methyl-morpholine / tetrahydrofuran / 38 °C / Inert atmosphere

7.1: hydrogenchloride / tetrahydrofuran; methanol / 2 h / 2 °C / pH 1.5 - 1.9

8.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 72 h / 20 °C

8.2: florosil / 0.17 h

9.1: sodium periodate / water; tetrahydrofuran / 2.5 h / 20 °C

10.1: sodium cyanoborohydride; acetic acid / ethanol / 2.33 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; lithium borohydride; water; pivaloyl chloride; sodium cyanoborohydride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; acetic acid; In tetrahydrofuran; methanol; ethanol; Isopropyl acetate; water; toluene; tert-butyl alcohol;

Reference yield:

: 943239-53-0
C₄₁H₆₆O₁₀Si₂

: 1269040-80-3
SY₆₃₄-70AP₁

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap; triethylamine / Isopropyl acetate / 3 h / 35 °C / Inert atmosphere

1.2: 0.25 h / 19.7 °C

2.1: water / acetic acid / methanol / 9 h / 50 - 55 °C

3.1: trifluoroacetic acid / toluene / -15 °C

3.2: 0.25 h / 5 °C / pH > 5

4.1: dmap; pivaloyl chloride; 4-methyl-morpholine / tetrahydrofuran / 38 °C / Inert atmosphere

5.1: hydrogenchloride / tetrahydrofuran; methanol / 2 h / 2 °C / pH 1.5 - 1.9

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; tetrahydrofuran / 72 h / 20 °C

6.2: florosil / 0.17 h

7.1: sodium periodate / water; tetrahydrofuran / 2.5 h / 20 °C

8.1: sodium cyanoborohydride; acetic acid / ethanol / 2.33 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; water; pivaloyl chloride; sodium cyanoborohydride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; acetic acid; In tetrahydrofuran; methanol; ethanol; Isopropyl acetate; water; toluene; tert-butyl alcohol;