3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide

Base Information

Chemical Name:3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide
CAS No.:1219119-08-0
Molecular Formula:C₂₂H₂₇ClN₄O₅
Molecular Weight:462.933
Hs Code.:

Synonyms:3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide

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Chemical Property of 3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide

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Technology Process of 3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide

There total 1 articles about 3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1072-98-6
5-chloro-2-pyridylamine

: 66636-17-7
N,N'-di-(tert-butoxycarbonyl)-3,4-diaminobenzoic acid

: 1219119-08-0
3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide

Guidance literature:: N,N'-di-(tert-butoxycarbonyl)-3,4-diaminobenzoic acid; With 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In dichloromethane; at 20 ℃; for 0.75h;

5-chloro-2-pyridylamine; With pyridine; In dichloromethane; at 20 ℃; for 1.5h;

Reference yield: 69.0%

: 1219119-08-0
3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide

: 1219119-09-1
3,4-diamino-benzoic acid (5-chloro-pyridine-2-yl)amide

Guidance literature:: 3,4-bis-tert-butoxycarbonylamino-benzoic acid (5-chloro-pyridine-2-yl)amide; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

With sodium hydroxide; In water; Cooling with ice;