methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate

Base Information

Chemical Name:methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate
CAS No.:1100155-33-6
Molecular Formula:C₁₆H₂₃FO₄
Molecular Weight:298.355
Hs Code.:

Synonyms:methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate

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Chemical Property of methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate

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Technology Process of methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate

There total 12 articles about methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1100155-31-4
(S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

: 1100155-33-6
methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 3h;

Reference yield:

: methyl (S,Z)-6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

: 1100155-33-6
methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 - 25 ℃; for 3h;

Reference yield:

: 1100155-27-8
(S)-6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-hydroxyethyl)hex-4-enoic acid

: 1100155-33-6
methyl (S)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)-6-hydroxyhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 3 h / 0 - 25 °C

2: sulfuric acid / 8 h / 25 °C

3: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 25 °C

With sulfuric acid; palladium 10% on activated carbon; hydrogen; sodium hydride; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2011.02.010