(S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

Base Information

Chemical Name:(S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate
CAS No.:1100155-31-4
Molecular Formula:C₂₃H₂₇FO₄
Molecular Weight:386.463
Hs Code.:

Synonyms:(S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

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Chemical Property of (S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

Chemical Property:

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Technology Process of (S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

There total 6 articles about (S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1100155-29-0
(S)-6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoic acid

: 1100155-31-4
(S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

Guidance literature:: With sulfuric acid; In water; at 20 ℃; for 8h;

Reference yield:

: 1100155-25-6
(3S,5R)-3-(4-(benzyloxy)but-2-enyl)-5-(4-fluorophenyl)dihydrofuran-2(3H)-one

: 1100155-31-4
(S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / 1,4-dioxane; water / 0.5 h / 25 °C

2: sodium hydride / tetrahydrofuran / 3 h / 0 - 25 °C

3: sulfuric acid / 8 h / 25 °C

With sulfuric acid; sodium hydride; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1016/j.bmcl.2011.02.010

Reference yield:

: 1100155-27-8
(S)-6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-hydroxyethyl)hex-4-enoic acid

: 1100155-31-4
(S)-methyl 6-(benzyloxy)-2-((R)-2-(4-fluorophenyl)-2-methoxyethyl)hex-4-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 3 h / 0 - 25 °C

2: sulfuric acid / 8 h / 25 °C

With sulfuric acid; sodium hydride; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2011.02.010