E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene

Base Information

Chemical Name:E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene
CAS No.:1371574-56-9
Molecular Formula:C₂₀H₂₂O₄
Molecular Weight:326.392
Hs Code.:

Synonyms:E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene

Suppliers and Price of E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene

There total 15 articles about E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1408062-17-8
E-1-[5-benzyloxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-benzyloxy-3-methoxyphenyl]ethene

: 1371574-56-9
E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene

: 1408062-21-4
1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethane

Guidance literature:: With cyclohexa-1,4-diene; palladium 10% on activated carbon; In ethanol; Reflux; Inert atmosphere;
DOI:10.1016/j.ejmech.2013.02.017

Reference yield:

: 1408062-17-8
E-1-[5-benzyloxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-benzyloxy-3-methoxyphenyl]ethene

: 1371574-56-9
E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene

Guidance literature:: With cyclohexa-1,4-diene; palladium 10% on activated carbon; In ethanol; at 80 ℃; for 4h; Inert atmosphere;

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 1371574-56-9
E-1-[5-hydroxy-3-(3-methylbut-2-enyloxy)phenyl]-2-[4-hydroxy-3-methoxyphenyl]ethene

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 2 h

2.1: palladium diacetate; N-ethylmorpholine; / xylene / 130 °C / Inert atmosphere

3.1: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

5.1: cyclohexa-1,4-diene / palladium 10% on activated carbon / ethanol / 4 h / 80 °C / Inert atmosphere

With cyclohexa-1,4-diene; potassium tert-butylate; water; sodium hydride; sodium hydroxide; N-ethylmorpholine;; palladium 10% on activated carbon; palladium diacetate; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; xylene; mineral oil;