5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine

Base Information

Chemical Name:5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine
CAS No.:869119-26-6
Molecular Formula:C₁₇H₂₃N₅O₂S
Molecular Weight:361.468
Hs Code.:

Synonyms:5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine

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Chemical Property of 5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine

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Technology Process of 5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine

There total 5 articles about 5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 869119-61-9
2-(4-methoxybenzylsulfanyl)-4-methylamino-6-morpholino pyrimidine

: 869119-26-6
5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine

Guidance literature:: 2-(4-methoxybenzylsulfanyl)-4-methylamino-6-morpholino pyrimidine; With acetic acid; sodium nitrite; In water; at 20 ℃; for 5h;

With sodium hydroxide; In water;

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 4h; under 760.051 Torr;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 869119-26-6
5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / N,N-dimethyl-formamide / 1.75 h / 100 °C

2.1: trichlorophosphate; N,N-dimethyl-aniline / 1.5 h / 100 °C

3.1: methanol / 20 °C

4.1: 80 °C

5.1: sodium nitrite; acetic acid / water / 5 h / 20 °C

5.3: 4 h / 760.05 Torr

With acetic acid; N,N-dimethyl-aniline; triethylamine; sodium nitrite; trichlorophosphate; In methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 86627-06-7
2-<(4-methoxybenzyl)thio>-4,6(1H,5H)-pyrimidinedione

: 869119-26-6
5-amino-2-(4-methoxybenzylsulfanyl)-6-methylamino-4-morpholinopyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate; N,N-dimethyl-aniline / 1.5 h / 100 °C

2.1: methanol / 20 °C

3.1: 80 °C

4.1: sodium nitrite; acetic acid / water / 5 h / 20 °C

4.3: 4 h / 760.05 Torr

With acetic acid; N,N-dimethyl-aniline; sodium nitrite; trichlorophosphate; In methanol; water;