2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate

Base Information

Chemical Name:2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate
CAS No.:1563184-90-6
Molecular Formula:C₁₄H₂₀BrN₃O₇S
Molecular Weight:454.299
Hs Code.:

Synonyms:2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate

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Chemical Property of 2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate

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Technology Process of 2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate

There total 6 articles about 2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1563184-94-0
((2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)azanediyl)bis(ethane-2,1-diyl)dimethanesulfonate

: 1563184-90-6
2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate

Guidance literature:: With lithium bromide; In acetone; at 20 ℃;

Reference yield:

: 7304-32-7
2-fluoro-5-nitrobenzoic acid

: 1563184-90-6
2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Reflux

1.2: 0.5 h / -10 - 20 °C

2.1: triethylamine / 1,4-dioxane / 55 °C

3.1: triethylamine / dichloromethane / 0.5 h / 0 - 20 °C

4.1: methanesulfonyl chloride; methanol / 0.33 h / 20 °C

5.1: lithium bromide / acetone / 20 °C

With methanol; thionyl chloride; methanesulfonyl chloride; triethylamine; N,N-dimethyl-formamide; lithium bromide; In 1,4-dioxane; dichloromethane; acetone;

Reference yield:

: 1563184-93-9
((4-nitro-2-((2-((tetrahydro-2H-pyran-2-yl)oxy)ethyl)carbamoyl)phenyl)azanediyl)bis(ethane-2,1-diyl)dimethanesulfonate

: 1563184-90-6
2-((2-bromoethyl)(2-((2-hydroxyethyl)carbamoyl)-4-nitrophenyl)amino)ethyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonyl chloride; methanol / 0.33 h / 20 °C

2: lithium bromide / acetone / 20 °C

With methanol; methanesulfonyl chloride; lithium bromide; In acetone;