[2-[2-[2-[2-Formyl-5-[3-(trifluoromethyl)-3H-diazirin-3-yl]phenoxy]ethoxy]ethoxy]ethyl]carbamic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:[2-[2-[2-[2-Formyl-5-[3-(trifluoromethyl)-3H-diazirin-3-yl]phenoxy]ethoxy]ethoxy]ethyl]carbamic acid 1,1-dimethylethyl ester
CAS No.:299931-13-8
Molecular Formula:C₂₀H₂₆F₃N₃O₆
Molecular Weight:461.438
Hs Code.:
Mol file:299931-13-8.mol

Synonyms:2-[2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy]-4-[3-(trifluoromethyl)-3H-diazirin-3-yl] benzaldehyde

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Chemical Property of [2-[2-[2-[2-Formyl-5-[3-(trifluoromethyl)-3H-diazirin-3-yl]phenoxy]ethoxy]ethoxy]ethyl]carbamic acid 1,1-dimethylethyl ester

Chemical Property:

Density:1.30±0.1 g/cm3 (20 oC 760 Torr)

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Technology Process of [2-[2-[2-[2-Formyl-5-[3-(trifluoromethyl)-3H-diazirin-3-yl]phenoxy]ethoxy]ethoxy]ethyl]carbamic acid 1,1-dimethylethyl ester

There total 2 articles about [2-[2-[2-[2-Formyl-5-[3-(trifluoromethyl)-3H-diazirin-3-yl]phenoxy]ethoxy]ethoxy]ethyl]carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 308085-25-8
2-hydroxy-4-[3-(trifluoromethyl)-3H-diazirin-3-yl] benzaldehyde

: 2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethyl bromide

: 299931-13-8
2-[2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy]-4-[3-(trifluoromethyl)-3H-diazirin-3-yl] benzaldehyde

Guidance literature:: With potassium carbonate; tetra-(n-butyl)ammonium iodide; In DMF (N,N-dimethyl-formamide); at 60 ℃; for 14h;

Reference yield:

: 205485-25-2
2-methoxy-4-<3-trifluoromethyl-3H-diazirin-3-yl>benzaldehyde

: 299931-13-8
2-[2-[2-(2-tert-butoxycarbonylaminoethoxy)ethoxy]ethoxy]-4-[3-(trifluoromethyl)-3H-diazirin-3-yl] benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / BBr₃ / CH₂Cl₂ / 1 h / 0 °C

2: 91 percent / K₂CO₃; nBu₄NI / dimethylformamide / 12 h / 60 °C

With boron tribromide; tetra-(n-butyl)ammonium iodide; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(01)00025-8