N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate

Base Information

Chemical Name:N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate
CAS No.:1352610-22-0
Molecular Formula:C₂₄H₂₁N₇*H₂O₄S
Molecular Weight:505.557
Hs Code.:

Synonyms:N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate

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Chemical Property of N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate

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Technology Process of N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate

There total 7 articles about N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1352609-09-6
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline

: 1352610-22-0
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate

Guidance literature:: With sulfuric acid; In ethanol; at 0 - 20 ℃;

Reference yield:

: 614750-82-2
1-(6-methylpyridin-2-yl)-2-[1,2,4]triazolo-[1,5-a]pyridin-6-yl-ethanone

: 1352610-22-0
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethyl sulfoxide; hydrogen bromide / 2 h / 60 - 70 °C

2.1: ammonium acetate / water; tert-butyl methyl ether; methanol / 3 h / 20 °C

2.2: pH 8

3.1: hydrogenchloride; water / 3 h / 70 °C

3.2: 0 °C

4.1: acetic acid / 1,2-dichloro-ethane / 2 h / 80 °C

4.2: 0 - 40 °C

5.1: sulfuric acid / ethanol / 0 - 20 °C

With hydrogenchloride; sulfuric acid; ammonium acetate; water; hydrogen bromide; acetic acid; dimethyl sulfoxide; In methanol; ethanol; tert-butyl methyl ether; water; 1,2-dichloro-ethane;

Reference yield:

: 356560-84-4
1-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-2-(6-methylpyridin-2-yl)ethane-1,2-dione

: 1352610-22-0
N-((4-([1,2,4]triazolo[1,5-a]pyridin-6-yl)-5-(6-methylpyridin-2-yl)-1H-imidazol-2-yl)methyl)-3-vinylaniline sulfate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium acetate / water; tert-butyl methyl ether; methanol / 3 h / 20 °C

1.2: pH 8

2.1: hydrogenchloride; water / 3 h / 70 °C

2.2: 0 °C

3.1: acetic acid / 1,2-dichloro-ethane / 2 h / 80 °C

3.2: 0 - 40 °C

4.1: sulfuric acid / ethanol / 0 - 20 °C

With hydrogenchloride; sulfuric acid; ammonium acetate; water; acetic acid; In methanol; ethanol; tert-butyl methyl ether; water; 1,2-dichloro-ethane;