3-bromo-5-methoxy phenyl benzoate

Base Information

• Chemical Name: 3-bromo-5-methoxy phenyl benzoate
• CAS No.: 260558-16-5
• Molecular Formula: C₁₄H₁₁BrO₃
• Molecular Weight: 307.144
• Mol file: 260558-16-5.mol

Synonyms:3-bromo-5-methoxy phenyl benzoate

Chemical Property of 3-bromo-5-methoxy phenyl benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-bromo-5-methoxy phenyl benzoate

There total 3 articles about 3-bromo-5-methoxy phenyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromoanisole (578-57-4) + (dibenzoyloxyiodo)benzene (6597-18-8) → 3-bromo-5-methoxy phenyl benzoate (260558-16-5)

Guidance literature:

With 2,4,6-trimethyl-pyridine; palladium(II) trifluoroacetate; at 100 ℃; for 4h; regioselective reaction; Sealed tube;

DOI:10.1016/j.tetlet.2016.11.055

Reference yield:

4-methoxyphenyl benzoate (1523-19-9) + acetic acid (64-19-7,77671-22-8) → 3-bromo-5-methoxy phenyl benzoate (260558-16-5)

Guidance literature:

DOI:10.1039/jr9270000074

Reference yield:

formic acid (64-18-6) + 4-methoxyphenyl benzoate (1523-19-9) + bromine (7726-95-6) → 3-bromo-5-methoxy phenyl benzoate (260558-16-5)

Guidance literature:

DOI:10.1039/jr9270000074

upstream raw materials:

formic acid

4-methoxyphenyl benzoate

bromine

acetic acid

Downstream raw materials:

3-bromo-4-methoxy-phenol