α-morpholine methyltrimethoxysilane

Base Information

• Chemical Name: α-morpholine methyltrimethoxysilane
• CAS No.: 154206-90-3
• Molecular Formula: C₈H₁₉NO₄Si
• Molecular Weight: 221.329
• Mol file: 154206-90-3.mol

Synonyms:α-morpholine methyltrimethoxysilane

Chemical Property of α-morpholine methyltrimethoxysilane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of α-morpholine methyltrimethoxysilane

There total 1 articles about α-morpholine methyltrimethoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(morpholinomethyl)hydrosilane (5625-96-7) + methanol (67-56-1) → 4-methyl-morpholine (109-02-4) + tetramethylorthosilicate (681-84-5) + α-morpholine methyltrimethoxysilane (154206-90-3)

Guidance literature:

In neat (no solvent); at 0 - 5 ℃; for 5h; Mechanism; Inert atmosphere;

DOI:10.1007/s10593-021-02910-w

Reference yield: 95.0%

tetraphenylethane-1,2-diol (464-72-2) + α-morpholine methyltrimethoxysilane (154206-90-3) → (morpholinomethyl)bis[tetraphenylethane-1,2-diolato(2-)]silicate

Guidance literature:

In acetonitrile; at 20 ℃; for 96h;

DOI:10.1002/1099-0682(200109)2001:9<2211::AID-EJIC2211>3.0.CO;2-K

Reference yield: 72.0%

1,1,3,3-tetraphenyldisiloxane-1,3-diol (1104-93-4) + toluene (108-88-3,15644-74-3,16713-13-6) + α-morpholine methyltrimethoxysilane (154206-90-3) → trans-2,8-bis(3-hydroxy-1,1,3,3-tetraphenyldisilan-1-yloxy)-2,8-bis(morpholinomethyl)-4,4,6,6,10,10,12,12-octaphenyl-cyclohexasiloxane toluene

Guidance literature:

In acetonitrile; at 20 ℃; for 24h;

DOI:10.1002/1099-0682(200109)2001:9<2211::AID-EJIC2211>3.0.CO;2-K

upstream raw materials:

(morpholinomethyl)hydrosilane

methanol

Downstream raw materials:

dimethoxy[(morpholino)methyl]phenylsilane

Refernces