2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2

Base Information

Chemical Name:2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2
CAS No.:451445-09-3
Molecular Formula:C₆₀H₇₄In₂
Molecular Weight:1024.89
Hs Code.:

2,6-(2,6-i-Pr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>InInC<sub>6</sub>H<sub>3</sub>-2,6-(C<sub>6</sub>H<sub>3</sub>-2,6-i-Pr<sub>2</sub>)2

Synonyms:2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2

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Chemical Property of 2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2

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Technology Process of 2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2

There total 1 articles about 2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.2%

: 12672-70-7
indium chloride

: 183293-75-6
2,6-bis(2,6-diisopropylphenyl)phenyllithium

: 451445-09-3
2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2

Guidance literature:: In toluene; under anaerobic and anhyd. conditions; soln. of Li compd. in toluene added dropwise to stirred slurry of InCl (molar ratio 1:1) in toluene at -78°C; warmed to 25°C overnight; pptd. over ca. 5 h; filtered; vol. of filtrate reduced under reduced pressure; crystd. at -20°C overnight;
DOI:10.1021/ja026285s

Reference yield: 65.0%

: 110-54-3
hexane

: 451445-09-3
2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2

: 10024-97-2
dinitrogen monoxide

: [(C₆H₃-2,6-(C₆H₃-2,6-(i-Pr)2)2)InO]2*0.5C₆H₁₄

Guidance literature:: In toluene; (N2); std. Schlenk technique; soln. of In compd. in toluene was treated with N2O for 2 min; evapd. (vac.); dissolved in hexane; concd.; stored at -18°C overnight;
DOI:10.1021/om900031v

Reference yield: 53.3%

: 451445-09-3
2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InInC₆H₃-2,6-(C₆H₃-2,6-i-Pr₂)2

: 1109-15-5
tris(pentafluorophenyl)borate

: 2,6-(2,6-i-Pr₂C₆H₃)2C₆H₃InB(C₆F₅)3

Guidance literature:: In toluene; under anaerobic and anhyd. conditions, in Schlenk tube; toluene added tomixt. of In compd. and B(C6F5)3 (molar ratio 1:2); stirred at 25.degree .c for 1 h; solvent evapd.; redissolved in hexane; vol. reduced; ppt. redissolved bywarming; cooled to 25°C over 3 h;
DOI:10.1021/ja026285s