[3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester

Base Information

Chemical Name:[3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester
CAS No.:156745-63-0
Molecular Formula:C₁₅H₂₇O₉P₃
Molecular Weight:444.295
Hs Code.:

Synonyms:[3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester

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Chemical Property of [3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester

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Technology Process of [3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester

There total 1 articles about [3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 18226-42-1
1,3,5-Tris(bromomethyl)benzene

: 121-45-9
phosphorous acid trimethyl ester

: 156745-63-0
[3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester

Guidance literature:: for 3h; Heating;
DOI:10.1021/ol9910924

Reference yield: 87.0%

: 2052-49-5
tetra(n-butyl)ammonium hydroxide

: 156745-63-0
[3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester

: [3,5-bis(hydroxymethoxyphosphorylmethyl)benzyl]phosphoric acid methyl ester tris(tetrabutylammonium) salt

Guidance literature:: With water; for 336000h; Heating;
DOI:10.1021/ol9910924

Reference yield: 74.0%

: 156745-63-0
[3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester

: [3,5-bis-(methoxy-hydroxy-phosphorylmethyl)-benzyl]-phosphonic acid monomethyl ester

Guidance literature:: [3,5-bis(dimethoxyphosphorylmethyl)benzyl]phosphoric acid dimethyl ester; With potassium hydroxide; water; for 17h; Heating / reflux;

With hydrogenchloride; In water; at 20 ℃; pH=1;