2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

Base Information

Chemical Name:2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole
CAS No.:1350440-45-7
Molecular Formula:C₄₁H₃₇ClN₆S
Molecular Weight:681.304
Hs Code.:

Synonyms:2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

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Chemical Property of 2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

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Technology Process of 2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

There total 2 articles about 2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350440-44-6
5-acetylthiomethyl-2-butyl-4-chloro-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

: 1350440-45-7
2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

Guidance literature:: With morpholine; 1,4-dithio-erythritol; In dichloromethane; at 20 ℃; for 72h;

Reference yield:

: 124751-00-4
2-Butyl-4-chloro-1-[[2'-[1-(triphenylmethyl)-1H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-1H-imidazole-5-methanol

: 1350440-45-7
2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Cooling with ice

1.2: 4 h / 20 °C

2.1: 1,4-dithio-erythritol; morpholine / dichloromethane / 72 h / 20 °C

With morpholine; 1,4-dithio-erythritol; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 299176-17-3
N-(2-nitro-5-chlorophenyl)-N-methylcarbamic acid t-butyl ester

: 1350440-45-7
2-butyl-4-chloro-5-mercaptomethyl-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

: 1350440-46-8
5-(3-(N-t-butoxycarbonyl-N-methylamino)-4-nitrophenylthiomethyl)-2-butyl-4-chloro-1-[2'-(1-triphenylmethyl-1H-tetrazol-5-yl)biphenyl-4-ylmethyl]-1H-imidazole

Guidance literature:: With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; mineral oil; at 20 - 70 ℃; for 7.75h; Inert atmosphere;