p-toluenesulphonyloxamoyl chloride

Base Information

• Chemical Name: p-toluenesulphonyloxamoyl chloride
• CAS No.: 101386-15-6
• Molecular Formula: C₉H₈ClNO₄S
• Molecular Weight: 261.686

Synonyms:p-toluenesulphonyloxamoyl chloride

Chemical Property of p-toluenesulphonyloxamoyl chloride

Chemical Property:

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Technology Process of p-toluenesulphonyloxamoyl chloride

There total 1 articles about p-toluenesulphonyloxamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxalyl dichloride (79-37-8) + toluene-4-sulfonamide (70-55-3) → p-toluenesulphonyloxamoyl chloride (101386-15-6)

Guidance literature:

DOI:10.1021/jo01032a025

Reference yield: 71.0%

2-amino-5-ethyl-1,3,4-thiadiazole (14068-53-2) + p-toluenesulphonyloxamoyl chloride (101386-15-6) → N-p-tolylsulfonyl-N'-(5-ethylthiadiazol-2-yl)oxamide

Guidance literature:

In acetonitrile; at 20 ℃; for 20h;

DOI:10.1002/(SICI)1526-4998(200003)56:3<218::AID-PS116>3.0.CO;2-9

Reference yield:

p-toluenesulphonyloxamoyl chloride (101386-15-6) → Tosyl isocyanate (4083-64-1)

Guidance literature:

With 1,2-dichloro-benzene; Heating;

DOI:10.1021/jo01032a025

upstream raw materials:

oxalyl dichloride

toluene-4-sulfonamide

Downstream raw materials:

Tosyl isocyanate

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