3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride

Base Information

Chemical Name:3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride
CAS No.:1613454-83-3
Molecular Formula:C₂₅H₂₄FN₆O*Cl
Molecular Weight:478.957
Hs Code.:

Synonyms:3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride

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Chemical Property of 3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride

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Technology Process of 3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride

There total 11 articles about 3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1613454-82-2
3,8-bis(tert-butoxycarbonylamino)-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridiniumiodide

: 1613454-83-3
3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 3h; Inert atmosphere;
DOI:10.1039/c3ob42379d

Reference yield:

: 51787-75-8
4,4'-dinitro-2-biphenylamine

: 1613454-83-3
3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride

Guidance literature:: Multi-step reaction with 10 steps

1: 24 h / Inert atmosphere; Reflux

2: ammonium formate; 20% palladium hydroxide-activated charcoal / methanol; ethyl acetate / 3 h / Inert atmosphere; Reflux

3: triethylamine / dichloromethane / 23 °C / Inert atmosphere

4: trichlorophosphate / 6 h / Inert atmosphere; Reflux

5: hydrogen bromide / 72 h / Inert atmosphere; Reflux

6: tert-butyl alcohol / 48 h / 23 °C / Inert atmosphere

7: potassium carbonate / toluene; acetone / 8 h / Inert atmosphere; Reflux

8: tetrahydrofuran / 120 h / Inert atmosphere; Reflux

9: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide / 23 °C / Inert atmosphere

10: hydrogenchloride / ethyl acetate / 3 h / Inert atmosphere

With hydrogenchloride; copper(ll) sulfate pentahydrate; 20% palladium hydroxide-activated charcoal; hydrogen bromide; ammonium formate; potassium carbonate; sodium L-ascorbate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;
DOI:10.1039/c3ob42379d

Reference yield:

: 1314081-04-3
di-tert-butyl [6-(4-hydroxyphenyl)phenanthridine-3,8-diyl]dicarbamate

: 1613454-83-3
3,8-diamino-6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methylphenanthridinium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / toluene; acetone / 8 h / Inert atmosphere; Reflux

2: tetrahydrofuran / 120 h / Inert atmosphere; Reflux

3: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide / 23 °C / Inert atmosphere

4: hydrogenchloride / ethyl acetate / 3 h / Inert atmosphere

With hydrogenchloride; copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1039/c3ob42379d