3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide

Base Information

• Chemical Name: 3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide
• CAS No.: 1314081-06-5
• Molecular Formula: C₃₃H₃₆N₃O₅*I
• Molecular Weight: 681.57

Synonyms:3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide

Chemical Property of 3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide

There total 9 articles about 3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate (1314081-05-4) + methyl iodide (74-88-4) → 3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide (1314081-06-5)

Guidance literature:

In tetrahydrofuran; for 120h; Inert atmosphere; Reflux;

DOI:10.1039/c3ob42379d

Reference yield:

4-methoxy-benzoyl chloride (100-07-2) → 3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide (1314081-06-5)

Guidance literature:

Multi-step reaction with 8 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

8: tetrahydrofuran

With hydrogen bromide; ammonium formate; potassium carbonate; trichlorophosphate; 20 % Pd(OH)2/C; In tetrahydrofuran; water; chlorobenzene; acetone;

Reference yield:

4,4'-dinitro-2-biphenylamine (51787-75-8) → 3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide (1314081-06-5)

Guidance literature:

Multi-step reaction with 8 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

8: tetrahydrofuran

With hydrogen bromide; ammonium formate; potassium carbonate; trichlorophosphate; 20 % Pd(OH)2/C; In tetrahydrofuran; water; chlorobenzene; acetone;

upstream raw materials:

di-tert-butyl 6-(4-(prop-2-ynyloxy)phenyl)phenanthridine-3,8-diyldicarbamate

methyl iodide

4-methoxy-benzoyl chloride

4,4'-dinitro-2-biphenylamine

Downstream raw materials:

di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate

C₂₅H₂₅FN₆O

[¹⁸F]6-(4-((1-(2-fluoroethyl)-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diamine

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