4-Oxa-1,2-diazaspiro[4.4]non-1-ene,3-methoxy-3-methyl-(9CI)

Base Information

Chemical Name:4-Oxa-1,2-diazaspiro[4.4]non-1-ene,3-methoxy-3-methyl-(9CI)
CAS No.:119393-19-0
Molecular Formula:C8H14 N2 O2
Molecular Weight:170.211
Hs Code.:
Mol file:119393-19-0.mol

Synonyms:4-Oxa-1,2-diazaspiro[4.4]non-1-ene,3-methoxy-3-methyl-(9CI)

Suppliers and Price of 4-Oxa-1,2-diazaspiro[4.4]non-1-ene,3-methoxy-3-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 4-Oxa-1,2-diazaspiro[4.4]non-1-ene,3-methoxy-3-methyl-(9CI)

Chemical Property:

PSA：43.18000
LogP:0.93040

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Oxa-1,2-diazaspiro[4.4]non-1-ene,3-methoxy-3-methyl-(9CI)

There total 3 articles about 4-Oxa-1,2-diazaspiro[4.4]non-1-ene,3-methoxy-3-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 67-56-1
methanol

: 1068-57-1
acetic acid hydrazide

: 120-92-3
cyclopentanone

: 119393-19-0
2-methoxy-2-methyl-3,4-diaza-1-oxa<4.4>spironon-3-ene

Guidance literature:: acetic acid hydrazide; cyclopentanone; In toluene; for 2h; Dean-Stark; Inert atmosphere; Reflux;

methanol; With [bis(acetoxy)iodo]benzene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201710445

Reference yield: 70.0%

: 67-56-1
methanol

: 28766-48-5
1-acetyl-2-(1-cyclopentylidene)hydrazine

: 119393-19-0
2-methoxy-2-methyl-3,4-diaza-1-oxa<4.4>spironon-3-ene

Guidance literature:: With lead(IV) acetate; at -10 ℃;
DOI:10.1021/jo00269a019

Reference yield:

: 120-92-3
cyclopentanone

: 119393-19-0
2-methoxy-2-methyl-3,4-diaza-1-oxa<4.4>spironon-3-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / benzene / Heating

2: 70 percent / Pb(OAc)4 / -10 °C

With lead(IV) acetate; In benzene;
DOI:10.1021/jo00269a019