(2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester

Base Information

Chemical Name:(2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester
CAS No.:197902-91-3
Molecular Formula:C₂₂H₂₃NO₅
Molecular Weight:381.428
Hs Code.:

Synonyms:(2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester

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Chemical Property of (2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester

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Technology Process of (2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester

There total 5 articles about (2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84688-11-9
(S)-2-(1,3-dioxoisoindolin-2-yl)-6-hydroxyhexanoic acid

: 197902-91-3
(2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Cs₂CO₃ / dimethylformamide / 2 h / Ambient temperature

2: 1.) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) CH₂Cl₂, -78 deg C, 5 min

3: CH₂Cl₂ / 0.5 h

With oxalyl dichloride; caesium carbonate; dimethyl sulfoxide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm980542f

Reference yield:

: 84688-13-1
(S)-2-phthalimido-6-hydroxyhexanoic acid, phenylmethyl ester

: 197902-91-3
(2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) CH₂Cl₂, -78 deg C, 5 min

2: CH₂Cl₂ / 0.5 h

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.1021/jm980542f

Reference yield:

: 100-39-0
benzyl bromide

: 197902-91-3
(2S)-2-phthalimido-6-hydroxyheptanoic acid, phenylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Cs₂CO₃ / dimethylformamide / 2 h / Ambient temperature

2: 1.) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) CH₂Cl₂, -78 deg C, 5 min

3: CH₂Cl₂ / 0.5 h

With oxalyl dichloride; caesium carbonate; dimethyl sulfoxide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm980542f