3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate

Base Information

Chemical Name:3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate
CAS No.:1276662-90-8
Molecular Formula:C₁₃H₁₇F₃O₅S₂
Molecular Weight:374.402
Hs Code.:

Synonyms:3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate

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Chemical Property of 3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate

Chemical Property:

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Technology Process of 3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate

There total 5 articles about 3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1276662-89-5
3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butan-1-ol

: 124-63-0
methanesulfonyl chloride

: 1276662-90-8
3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 1276662-82-8
3-methyl-3-((3-(trifluoromethyl)phenyl)thio)butanoic acid

: 1276662-90-8
3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: Oxone / water; methanol / 16 h / 20 °C

2.1: acetyl chloride / 2 h / 0 °C / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

With Oxone; lithium aluminium tetrahydride; triethylamine; acetyl chloride; In tetrahydrofuran; methanol; water;

Reference yield:

: 1276662-86-2
3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butanoic acid

: 1276662-90-8
3-methyl-3-((3-(trifluoromethyl)phenyl)sulfonyl)butyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetyl chloride / 2 h / 0 °C / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: triethylamine / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; acetyl chloride; In tetrahydrofuran;