1,3,5-Trimethyl-2,4,6-triphenyl-borazin

Base Information

Chemical Name:1,3,5-Trimethyl-2,4,6-triphenyl-borazin
CAS No.:909-21-7
Molecular Formula:C₂₁H₂₄B₃N₃
Molecular Weight:350.875
Hs Code.:

Synonyms:1,3,5-Trimethyl-2,4,6-triphenyl-borazin

Suppliers and Price of 1,3,5-Trimethyl-2,4,6-triphenyl-borazin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,3,5-Trimethyl-2,4,6-triphenyl-borazin

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3,5-Trimethyl-2,4,6-triphenyl-borazin

There total 28 articles about 1,3,5-Trimethyl-2,4,6-triphenyl-borazin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 920-68-3
heptamethyldisilazane

: 873-51-8
phenylborondichloride

: 909-21-7
1,3,5-Trimethyl-2,4,6-triphenyl-borazin

Guidance literature:: In benzene; byproducts: (CH3)3SiCl; absence of moisture; addn. of silylamine to borane derivative (during 4h, cooling in ice/EtOH, stirring), slow warming to room temp. (overnight); distn. of Me3SiCl (50-55°C, atmospheric pressure), repeated fractional distn.;

Reference yield: 63.0%

: 976-29-4
1,3,5-triphenyl-borazine

: 75-16-1
methylmagnesium bromide

: 2622-05-1
allylmagnesium bromide

: 126583-49-1
(allyl)(dimethyl)(1,3,5-triphenyl)borazine

: 909-21-7
1,3,5-Trimethyl-2,4,6-triphenyl-borazin

Guidance literature:: In diethyl ether; N2 atmosphere; addn. of soln. of MeMgBr in Et2O to soln. of B-compd. in Et2O(room temp.), stirring (1 h, room temp.), addn. of allylmagnesium chloride, stirring (overnight, room temp.); filtn., removal of solvent, extn. (hexane), filtn., removal of solvent, recrystn. (hexane); elem. anal.;

Reference yield: 51.0%

: 703-86-6
2,4,6-trichloro-1,3,5-trimethylborazine

: 1826-67-1
vinyl magnesium bromide

: 100-58-3
phenylmagnesium bromide

: 126583-45-7
(vinyl)(diphenyl)(1,3,5-trimethyl)borazine

: 909-21-7
1,3,5-Trimethyl-2,4,6-triphenyl-borazin

Guidance literature:: In diethyl ether; N2 atmosphere; addn. of soln. of PhMgBr in Et2O to soln. of B-compd. in Et2O(room temp.), stirring (1 h, room temp.), addn. of vinylmagnesium bromide, stirring (overnight, room temp.); removal of solvent, extn. (hot hexane), crystn. (hexane-CH2Cl2); elem. anal.;