703-86-6Relevant articles and documents
Butcher,Gerrard
, p. 823,828 (1965)
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Ryschkewitsch et al.
, p. 4515 (1958)
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METHOD FOR PRODUCING TRICHLOROBORAZINE COMPOUND AND METHOD FOR PRODUCING ALYKYLBORAZINE COMPOUND
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Page/Page column 14, (2008/06/13)
PROBLEM TO BE SOLVED: To provide a means for efficiently purifying a synthesized trichloroborazine compound. SOLUTION: The subject method for producing the trichloroborazine compound comprises the following steps. A step of reacting boron trichloride with an amine compound represented by R1NH3X (wherein, R1 is hydrogen atom or an alkyl group; and X is a halogen atom) in a solvent and producing the trichloroborazine compound represented by formula 2 (wherein, R2s may each the same or different and are each hydrogen atom or an alkyl group), a step of filtering the reaction solution and affording a filtrate and a step of distilling off the solvent from the filtrate and providing a solid substance composed of the trichloroborazine compound.
Synthesis and thermal decomposition studies of some novel dimethyl(phenyl)silyl-substituted aminoboranes
Bowser, James R.,Marohn, Kristina F.,Gilbert, Stephanie R.,Robbins, Andrea M.
, p. 1559 - 1566 (2008/10/09)
Reactions of chloro(dimethyl)phenylsilane with primary amines have been used to obtain a series of compounds having the general formula C6H5(CH3)2SiNHR. The anions of those species are readily prepared, and may be reacted with trichloroborane or dichlorophenylborane to give the corresponding silylaminoboranes, C6H5(CH3)2SiN(R)B(X)Cl (X = Cl, Ph). The thermal properties of these silylaminoboranes have been probed using thermogravimetric analysis. The first step in their thermal degradation involves elimination of C6H5(CH3)2SiCl.