Ethanol, 2-(3-pyridinyloxy)- (9CI)

Base Information

• Chemical Name: Ethanol, 2-(3-pyridinyloxy)- (9CI)
• CAS No.: 119967-49-6
• Molecular Formula: C7H9NO2
• Molecular Weight: 139.154
• Hs Code.: 2933399090
• Mol file: 119967-49-6.mol

Synonyms:2-(3-Pyridinyloxy)ethanol;

Chemical Property of Ethanol, 2-(3-pyridinyloxy)- (9CI)

Chemical Property:

• Appearance/Colour: colorless or light yellow liquid
• Vapor Pressure: 0.00298mmHg at 25°C
• Melting Point: 98-99℃
• Refractive Index: 1.528
• Boiling Point: 272.4 °C at 760 mmHg
• Flash Point: 118.5 °C
• PSA: 42.35000
• Density: 1.153 g/cm³
• LogP: 0.45270
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

2-(Pyridin-3-yloxy)ethan-1-ol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanol, 2-(3-pyridinyloxy)- (9CI)

There total 7 articles about Ethanol, 2-(3-pyridinyloxy)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-Bromopyridine (626-55-1,163928-56-1) + ethylene glycol (107-21-1) → 2-[(3-pyridinyl)oxy]ethanol (119967-49-6)

Guidance literature:

With potassium carbonate; copper dichloride; at 130 ℃; for 20h; Inert atmosphere; Schlenk technique;

DOI:10.1039/c4ob00649f

Reference yield: 86.0%

3-pyridyloxyethyl tetrahydro-2H-pyran-2-yl ether → 2-[(3-pyridinyl)oxy]ethanol (119967-49-6)

Guidance literature:

In tetrahydrofuran; water; acetic acid;

Reference yield: 72.0%

3-HYDROXYPYRIDINE (109-00-2) + [1,3]-dioxolan-2-one (96-49-1) → 2-[(3-pyridinyl)oxy]ethanol (119967-49-6)

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 86 ℃; for 20h;

upstream raw materials:

3-Bromopyridine

ethylene glycol

oxirane

3-HYDROXYPYRIDINE

Downstream raw materials:

3-vinyloxypyridine

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