diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate

Base Information

Chemical Name:diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate
CAS No.:864871-39-6
Molecular Formula:C₂₀H₂₉NO₇
Molecular Weight:395.453
Hs Code.:

Synonyms:diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate

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Chemical Property of diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate

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Technology Process of diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate

There total 4 articles about diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 105-53-3
diethyl malonate

: 741259-87-0
tert-butyl (4-methoxyphenyl)(phenylsulfonyl)methylcarbamate

: 864871-39-6
diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate

Guidance literature:: With potassium carbonate; In acetonitrile; at 30 ℃; for 24h;
DOI:10.1080/00397910600602537

Reference yield: 82.0%

: di-tert-butyl ((4-methoxyphenyl)methylene)dicarbamate

: 105-53-3
diethyl malonate

: 864871-39-6
diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 24h; Molecular sieve;
DOI:10.1002/anie.201300231

Reference yield:

: 105-53-3
diethyl malonate

: 365441-82-3
N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-4-methoxybenzylamine

: 864871-39-6
diethyl 2-(1-(N-tert-butoxycarbonylamino)-1-(4-methoxyphenyl)methyl)malonate

Guidance literature:: diethyl malonate; With sodium hydride; In tetrahydrofuran; cooling;

N-(tert-butoxycarbonyl)-α-(4-methylphenylsulfonyl)-4-methoxybenzylamine; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2005.04.077