10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one

Base Information

Chemical Name:10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one
CAS No.:1018386-80-5
Molecular Formula:C₃₀H₂₇F₃N₂O₄
Molecular Weight:536.551
Hs Code.:

Synonyms:10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one

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Chemical Property of 10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one

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Technology Process of 10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one

There total 3 articles about 10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1217552-36-7
C₃₀H₂₉F₃N₂O₄

: 1018386-80-5
10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one

Guidance literature:: With dihydrogen peroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water; at 20 ℃;
DOI:10.1055/s-0029-1218387

Reference yield: 86.0%

: 64369-54-6
7-(dimethylamino)-4-hydroxy-2H-1-benzopyran-2-one

: 1217552-34-5
6-methoxy-3,3-dimethyl-2-(4-trifluoromethyl)phenyl-1,2,3,4-tetrahydroquinolin-4-ol

: 1018386-80-5
10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one

Guidance literature:: With toluene-4-sulfonic acid; In 1,2-dichloro-ethane; for 6h; Reflux;
DOI:10.1055/s-0029-1218387

Reference yield: 67.0%

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 64369-54-6
7-(dimethylamino)-4-hydroxy-2H-1-benzopyran-2-one

: 104-94-9
4-methoxy-aniline

: 78-84-2
isobutyraldehyde

: 1018386-80-5
10-methoxy-6-(4-trifluoromethyl)phenyl-6,12-isopropano-6H,12H,13H-[1]-benzopyrano[4,3-d][1,3]-benzooxazocin-7-dimethylamino-13-one

Guidance literature:: 4-Trifluoromethylbenzaldehyde; 4-methoxy-aniline; isobutyraldehyde; With ytterbium(III) triflate; In 1,2-dichloro-ethane; at 20 ℃; for 12h;

7-(dimethylamino)-4-hydroxy-2H-1-benzopyran-2-one; In 1,2-dichloro-ethane; for 3h; Reflux;
DOI:10.1055/s-0029-1218387