6-mesyloxy-Nb-trifluoroacetyltryptamine

Base Information

• Chemical Name: 6-mesyloxy-Nb-trifluoroacetyltryptamine
• CAS No.: 259534-81-1
• Molecular Formula: C₁₃H₁₃F₃N₂O₄S
• Molecular Weight: 350.318

Synonyms:6-mesyloxy-Nb-trifluoroacetyltryptamine

Chemical Property of 6-mesyloxy-Nb-trifluoroacetyltryptamine

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Technology Process of 6-mesyloxy-Nb-trifluoroacetyltryptamine

There total 2 articles about 6-mesyloxy-Nb-trifluoroacetyltryptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

1,2,3-trimethoxybenzene (634-36-6) + methanesulfonyl chloride (124-63-0) + 1-hydroxy-Nb-trifluoroacetyltryptamine (180910-54-7) → N-(2-(1H-indol-3-yl)ethyl)-2,2,2-trifluoroacetamide (319-76-6) + (3a,8a-cis)-1,2,3,3a,8,8a-hexahydro-1-trifluoroacetyl-3a-(2,3,4-trimethoxyphenyl)pyrrolo[2,3-b]indole + (3a,8a-cis)-1,2,3,3a,8,8a-hexahydro-1-trifluoroacetyl-3a-[3-(Nb-trifluoroacetyl)aminoethylindol-1-yl]pyrrolo[2,3-b]indole + 1-trifluoroacety-2,3-dihydropyrrolo<2,3-b>indole + 6-mesyloxy-Nb-trifluoroacetyltryptamine (259534-81-1)

Guidance literature:

With triethylamine; In chloroform; at 0 ℃; for 1h;

DOI:10.3987/COM-16-S(S)53

Reference yield: 8.0%

methanesulfonyl chloride (124-63-0) + 1-hydroxy-Nb-trifluoroacetyltryptamine (180910-54-7) + phenol (108-95-2,27073-41-2) → N-(2-(1H-indol-3-yl)ethyl)-2,2,2-trifluoroacetamide (319-76-6) + (3a,8a-cis)-1,2,3,3a,8,8a-hexahydro-1-trifluoroacetyl-3a-[3-(Nb-trifluoroacetyl)aminoethylindol-1-yl]pyrrolo[2,3-b]indole + (3a,8a-cis)-1,2,3,3a,8,8a-hexahydro-3a-(4-hydroxyphenyl)-1-trifluoroacetylpyrrolo[2,3-b]indole + (3a,8a-cis)-1,2,3,3a,8,8a-hexahydro-3a-(2-hydroxyphenyl)-1-trifluoroacetylpyrrolo[2,3-b]indole + 6-mesyloxy-Nb-trifluoroacetyltryptamine (259534-81-1)

Guidance literature:

With triethylamine; In chloroform; at 0 ℃; for 1h;

DOI:10.3987/COM-16-S(S)53

upstream raw materials:

1,2,3-trimethoxybenzene

methanesulfonyl chloride

1-hydroxy-Nb-trifluoroacetyltryptamine

phenol

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