1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone

Base Information

Chemical Name:1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone
CAS No.:143337-95-5
Molecular Formula:C₂₂H₂₅NO₃
Molecular Weight:351.445
Hs Code.:

Synonyms:1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone

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Chemical Property of 1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone

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Technology Process of 1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone

There total 1 articles about 1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1224594-30-2
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-benzyloxypropanone

: 143337-95-5
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone

Guidance literature:: With 1% Pd/C; hydrogen; In ethanol; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2010.01.020

Reference yield: 88.0%

: 143337-95-5
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone

: 143337-96-6
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-bromopropanone

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1016/j.bmc.2010.01.020

Reference yield: 84.0%

: 143337-95-5
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone

: 507-09-5
tiolacetic acid

: 1085743-72-1
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -10 - 20 ℃;
DOI:10.1016/j.bmc.2010.01.020