1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone

Base Information

Chemical Name:1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone
CAS No.:1085743-72-1
Molecular Formula:C₂₄H₂₇NO₃S
Molecular Weight:409.549
Hs Code.:

Synonyms:1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone

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Chemical Property of 1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone

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Technology Process of 1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone

There total 2 articles about 1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₂₁H₂₃NSO₃

: 77-76-9
2,2-dimethoxy-propane

: 1085743-72-1
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2008.09.044

Reference yield: 84.0%

: 143337-95-5
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-hydroxylpropanone

: 507-09-5
tiolacetic acid

: 1085743-72-1
1-[2,2-dimethyl-8,8a-dihydro-3aH-indeno[(1S,2R)-1,2]-oxazol-3-yl]-(2R)-benzyl-3-acetylthiopropanone

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -10 - 20 ℃;
DOI:10.1016/j.bmc.2010.01.020